Nov 7 2023: This sample is the subject of a case report published in Journal of Forensic Sciences in Aug 2023, which identifies the previously unidentified substances. Summary below in Note.
Unidentified Substance #1: 3 parts
Unidentified Substance #2: 2 parts
Unidentified Substance #3: 15 parts
Unidentified Substance #4: 1 parts
Unidentified Substance #5: 2 parts
Unidentified Substance #6: 7 parts
unid 4: Unconfirmed (Lowest intensity peak), tentatively identified as being from a dichloroacetylchloride impurity in the chloroacetylchloride that produced N-(2-benzoyl-4-chlorophenyl)-2,2-dichloroacetamide (unid 3).
Sep 9 2022: According to one chemist, unidentified substance #1 is similar to 2-Amino-5-Chlorbenzophenone [CAS #719-59-5)], and #2 is similar to N-(2-benzoyl-4-chlorophenyl)acetamide [CAS# 13788-59-5] (thank you, Y.).
Jun 17 2022: Sucrose octaacetate matched for Unidentified #6. The DrugsData lab does not normally identify and report sugars. This version of sucrose is a bittering agent used in commercial products to reduce accidental ingestion. This is a special case, please do not ask us to identify simple sugars and salts.
Update Jan 29, 2021: We have re-attempted to identify these and found no matches with updated libraries and hundreds of new reference standards added to our library since the first analysis. We will attempt again in the future.
Unidentifed Substances
This sample contains an unidentified chemical. We do not have a matching substance in our lab's internal database and have not yet been able to identify the chemical(s).
We need the help of outside expert analytical chemists and drug geeks to determine what substance matches the mass spectrum (MS) fingerprint.
The lab's GC/MS graphs can be viewed by clicking on the thumbnails on this page.
Please use our contact form and include the DrugsData ID (8355) or this URL along with any communications.
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Unidentified Substance #1: 3 parts
Unidentified Substance #2: 2 parts
Unidentified Substance #3: 15 parts
Unidentified Substance #4: 1 parts
Unidentified Substance #5: 2 parts
Unidentified Substance #6: 7 parts
Details:
unid 1: 2-amino-5-chlorobenzophenone
unid 2: N-(2-benzoyl-4-chlorophenyl)acetamide
unid 3 (major constituent): N-(2-benzoyl-4-chlorophenyl)-2-chloroacetamide
unid 4: Unconfirmed (Lowest intensity peak), tentatively identified as being from a dichloroacetylchloride impurity in the chloroacetylchloride that produced N-(2-benzoyl-4-chlorophenyl)-2,2-dichloroacetamide (unid 3).
unid 5: 2-(2-benzoyl-4-chloroanilino)-2-oxoethyl acetate
unid 6: sucrose octaacetate (a safe bittering agent)
Jun 17 2022: Sucrose octaacetate matched for Unidentified #6. The DrugsData lab does not normally identify and report sugars. This version of sucrose is a bittering agent used in commercial products to reduce accidental ingestion. This is a special case, please do not ask us to identify simple sugars and salts. Update Jan 29, 2021: We have re-attempted to identify these and found no matches with updated libraries and hundreds of new reference standards added to our library since the first analysis. We will attempt again in the future.
We need the help of outside expert analytical chemists and drug geeks to determine what substance matches the mass spectrum (MS) fingerprint. The lab's GC/MS graphs can be viewed by clicking on the thumbnails on this page.
Please use our contact form and include the DrugsData ID (8355) or this URL along with any communications.